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KO50001004-00120045-0014  
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Title
Title Hot-press sintering of precious metals and glass beads  
Kana  
Romanization  
Other Title
Title  
Kana  
Romanization  
Creator
Name 坂田, 亮  
Kana サカタ, マコト  
Romanization Sakata, Makoto  
Affiliation Lecturer at Keio University  
Affiliation (Translated)  
Role  
Link  
Edition
 
Place
東京  
Publisher
Name 慶応義塾大学藤原記念工学部  
Kana ケイオウ ギジュク ダイガク フジワラ キネン コウガクブ  
Romanization Keio gijuku daigaku Fujiwara kinen kogakubu  
Date
Issued (from:yyyy) 1959  
Issued (to:yyyy)  
Created (yyyy-mm-dd)  
Updated (yyyy-mm-dd)  
Captured (yyyy-mm-dd)  
Physical description
 
Source Title
Name Proceedings of the Fujihara Memorial Faculty of Engineering Keio University  
Name (Translated)  
Volume 12  
Issue 45  
Year 1959  
Month  
Start page 68(14)  
End page 98(44)  
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Abstract
In order to study the fundamental mechanism of hot-press sintering, spherical beads of platinum, gold, 30-70 Au-Ag alloy and glass of equal sizes are sintered in a small cylindrical vessel under compressive load. The relations among the diameter of bead, load, sintering time and temperature (the temperature for the beginning of sintering) are determined by the testing method deviced by the author. The values of diameters of beads tested are mainly 0.85 mm, and for investigation of particle size effect 1.35 and 0.45 mm diameters are also used.
The rate of lowering of "the lowest sintering temperature" with the increase of load keeping the sintering time and the radius of bead constant has a maximum value in the range of recrystallization temperature of each metal or softening point of glass.
By the theoretical formula on the adhered area of glass, it is shown that the viscous flow is the rate-determining mechanism in hot-press sintering of glass.
The activation energy to effect hot-press sintering changes with temperature and load. It becomes smaller with temperature, but has a minimum value within the range of recrystallization temperature of each metal or softening point of glass, and then it becomes larger.
It is shown by this report that the recrystallization phenomena plays a prime role in hot-press sintering.
 
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NDC
 
Note
The twentieth anniversary memorial volume
 
Language
英語  
Type of resource
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Genre
Departmental Bulletin Paper  
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Last modified date
Oct 21, 2014 10:37:06  
Creation date
Oct 21, 2014 10:37:06  
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History
 
Index
/ Public / Faculty of Science and Technology / Keio Science and Technology Reports / 12(1959) / 12(45) 1959
 
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