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KAKEN_18H02040seika.pdf
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Title |
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高分子破壊現象プローブのための動的テラヘルツ劣化観察装置の開発
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Kana |
コウブンシ ハカイ ゲンショウ プローブ ノ タメ ノ ドウテキ テラヘルツ レッカ カンサツ ソウチ ノ カイハツ
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Kōbunshi hakai genshō purōbu no tame no dōteki teraherutsu rekka kansatsu sōchi no kaihatsu
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Development of time-dependent stain observation system for macromolecular destruction phenomenon probed by terahertz spectroscopy
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渡邉, 紳一
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ワタナベ, シンイチ
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Watanabe, Shin'ichi
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慶應義塾大学・理工学部 (矢上) ・教授
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Research team head
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科研費研究者番号 : 10376535
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2021
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科学研究費補助金研究成果報告書
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2020
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プラスチックの結晶化やゴムの応力軟化など、高分子材料の物性変化を動的に捉えることができるテラヘルツ分光計測装置を開発した。同装置を用いて高分子ポリ乳酸薄膜試料の加熱実験をおこない、ガラス転移や結晶化前後におけるテラヘルツ誘電応答の時間変化を捉えることに成功した。また、黒色ゴム試料の延伸に伴うテラヘルツ周波数領域の誘電応答の変化を調べ、試料内部に含有されているカーボンブラック凝集体の形状変化を推測することにも成功した。
We have developed a terahertz spectroscopy system to dynamically capture the changes in physical properties of polymeric materials, such as crystallization of plastics and stress softening of rubber. We succeeded in capturing temporal changes of terahertz dielectric responses of polylactic acid film sample before and after the glass transition and crystallization after heating the sample. We also succeeded in inferring the shape change of carbon black aggregates contained in a rubber sample from a dielectric response change in terahertz frequency region caused by stretching the sample.
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研究種目 : 基盤研究 (B) (一般)
研究期間 : 2018~2020
課題番号 : 18H02040
研究分野 : 光物性物理学
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